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MH2000 Experimental Methods 6.0 hp

Course memo Spring 2022-61502

Version 1 – 07/10/2022, 9:28:33 AM

Course offering

Spring 2022-1 (Start date 18/01/2022, English)

Language Of Instruction

English

Offered By

ITM/Materials Science and Engineering

Course memo Spring 2022

Course presentation

This course is intended to give an overview of common experimental methods used in the laboratory in materials science.

Diverse areas are covered, including scanning electron microscopy (SEM), x-ray diffraction (XRD), measurement of thermophysical properties, and thermodynamic and kinetic measurement techniques. Emphasis will also be on analysing experimental data with respect to quantifying uncertainties in measurement.

This is a hands-on course with some time being spent in the lab to become familiar with the different methods.

Headings denoted with an asterisk ( * ) is retrieved from the course syllabus version Spring 2020

Content and learning outcomes

Course contents

  • Frontline techniques in analysis and characterisation of materials (transmission electron microscopy, x-ray diffraction, scanning electron microscope, optical microscope)

  • Experimental conditions (high temperature furnaces, temperature control, gas phase, holding and refractory materials, other conditions)

  • Thermodynamic studies (calorimetry, thermal analysis, electromotive force, phase diagram studies, equilibrium and quenching, gas-condensed phase equilibria)

  • Kinetic studies (gravimetric analysis, electromotive force)

  • Physical properties (thermal and electrical conductivity, viscosity, surface and interfacial tension, density)

  • Experimental uncertainty analysis (types of error, standard methods for expressing error, measurement of error, propagation of determinate errors)

Intended learning outcomes

After completing the course the student should be able to:

  • Describe modern experimental methods in materials physics and chemistry.

  • Judge the precision and accuracy of the measurements.

  • Name the limitations of the respective techniques.

  • Choose the right technique to address specific material physics and chemistry questions.

Preparations before course start

Literature

No information inserted

Examination and completion

Grading scale

A, B, C, D, E, FX, F

Examination

  • LABA - Laboratory Work, 1.0 credits, Grading scale: P, F
  • LABB - Laboratory Work, 1.0 credits, Grading scale: P, F
  • TENA - Written examination, 4.0 credits, Grading scale: A, B, C, D, E, FX, F

Based on recommendation from KTH’s coordinator for disabilities, the examiner will decide how to adapt an examination for students with documented disability.

The examiner may apply another examination format when re-examining individual students.

The section below is not retrieved from the course syllabus:

Laboratory Work ( LABA )

Laboratory Work ( LABB )

Written examination ( TENA )

Ethical approach

  • All members of a group are responsible for the group's work.
  • In any assessment, every student shall honestly disclose any help received and sources used.
  • In an oral assessment, every student shall be able to present and answer questions about the entire assignment and solution.

Further information

No information inserted

Round Facts

Start date

18 Jan 2022

Course offering

  • Spring 2022-61502

Language Of Instruction

English

Offered By

ITM/Materials Science and Engineering

Contacts