In this practical laboratory course, a study of different parameters affecting the outcome for energy and environmental related processes will be carried out in a laboratory scale. The skills and knowledge gained in such studies are useful by analogy when solving problems that are typical for the chemical industry or research. The laboratory work to be performed is mainly ascribed to either homogeneous or heterogeneous catalysis, different preparation steps of catalysts, application on porous electrodes or other reactor formulations, or in purification methods. The laboratory requires study and measurement of flow rates of gases or liquids, temepartures, separation techniques, electrochemical assessments as well as other characterisation methods for gases, liquids and solids.
For the analytical work basic knowledge in mass and energy balances as well as kinetic models for calculation of chemical reactors as well as electrochemical systems are required. An introduction to factorial and experimental process design as useful statistical principles and methods for practical application in process optimization will also be covered during the course. Main emphasis on the design of experiments related to various factors affecting product yield, purity, etc. are of special interest for analytical work. The course is an exercise in process development, optimization and integration with analysis, planning and evaluation of the results obtained for the particular project task. The examination is a result of the experimental work, submission of a thorough final report and an oral presentation at the end in a seminar.